Filtration, Solid phase extraction

Filtration is accelerated either with pressure or with the aid of vacuum. The vacuum regulation and ultimate vacuum requirements are generally low. If it is filtered at 80 mbar, 92% of the atmospheric pressure is available as the driving force for filtration. Excess vacuum (e. g., from rotary vane pumps) can even cause evaporation of solvents instead of just liquid flow.

 

Process requirements

  • very modest ultimate vacuum, no more than average requirements
  • adequate vacuum flow rate, depending on the filter size, leak rate, condition of the filter cake, and whether a filtration manifold may be used to operate more than one filter at a time
  • simple, manual vacuum regulation

Demands made of the vacuum pump

  • single- or two-stage diaphragm pumps with as much as 70 or 7 mbar ultimate vacuum are ideal
  • excellent chemical and condensate compatibility for filtration or extraction of samples containing solvents
  • pump protection from particles and droplets of liquid with a suction-side separator (AK)
  • an exhaust condenser to minimize pollution of the environment and laboratory air from solvent vapors
  • chemistry pumping units that are equipped with electronic vacuum controllers shut off pump when filtration is complete

 

 

Recommended systems


 

Recommended systems

Down to 7 mbar

Down to 70 mbar

for corrosive gases


MZ 2C NT

MZ 2C NT +AK+M+D

MZ 2C NT +AK SYNCHRO+EK

ME 1C

ME 2C

ME 4C NT

for non-corrosive gases


MZ 2 NT

ME 1

ME 2

ME 4R NT